Image:Air-free filtration.svg

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[edit] Summary

Description

Air-free filtration


Apparatus:

a = receiving Schlenk flask (pink joint)

b = glass filter sinter/frit

c = filter stick

d = sealing bulb

e = suspension containing Schlenk flask (blue joint)

f = stopper

Method

1 = Dry apparatus and place under vacuum.

2 = Place filter stick and receiving flask (pink joint) on suspension containing flask (blue joint). Solution (blue) precipitate (green).

3 = Invert kit, light vacuum applied to lower flask, top flask sealed. Liquid passes through sinter. Precipitate trapped on sinter. Optionally, the precipitate can be washed with fresh solvent.

4 = Filtration complete, remove vacuum and fill with inert gas from top Schlenk flask

5 = Remove filter stick to obtain filtered solution (blue).

(Note if precipitate is required this can be collect either in a glove box or by washing a solvent through filter stick that will dissolve precipitate.)

Source

Re-drawn from work by Quantockgoblin

Date

7 Jun 2008

Author

Sashme

Permission
(Reusing this image)
Public domain I, the copyright holder of this work, hereby release it into the public domain. This applies worldwide.

In case this is not legally possible:
I grant anyone the right to use this work for any purpose, without any conditions, unless such conditions are required by law.


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Other versions Image:Air-free filtration.png

File history

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Date/TimeDimensionsUserComment
current05:59, 9 June 20081,202×579 (222 KB)Slashme (Fix amount of filtrate.)
09:18, 7 June 20081,202×579 (221 KB)Slashme (== Summary == {{Information |Description= Air-free filtration <U>Apparatus</U>: a = receiving Schlenk flask (pink joint) b = glass filter sinter/frit c = filter stick d = sealing bulb e = suspension containing Schlenk flask (blue joint) f)
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